1.1. J … Product Name: Ammonium Niobate(V) Oxalate Hydrate Product Number: All applicable American Elements product codes, e.g. Ammonium Oxalate, Saturated Solution: Show More Show Less: Safety and Handling GHS H Statement Solution is not hazardous. Record keeping and sample retention of all produced lots ensure product consistency and complete traceability. SCHEMBL36397. DTXSID50889443. Please make sure the Catalog Number and Lot Number are entered and click the Enter button. For additional information, please contact Customer Service at 800-813-1514 or, We are happy to provide Certificates of Analysis for our chemical products. They react as acids to neutralize bases. Evaporate the solution to ~ 1 ml, add 2 ml of H2SO4 (1 + 1), and heat to white fumes. CHEBI:91241. Belongs to the Following Reactive Group(s) Take 200 gm of ferric ammonium sulfate [FeCH4NO8S2] and dissolve in 300 ml water in a 500 ml beaker. Let cool, rinse the walls of the crucible with water and heat to fumes again. Later, they found that the contaminants were cyanuric acid and, Appendix 1. Acetate Buffer TS —Dissolve 320 g of ammonium acetate in 500 mL of water, add 5 mL of glacial acetic acid, dilute with water to 1000.0 mL, and mix. The pectins can be extracted with dilute acid, e.g. Add 100 ml of strong ammonium hydroxide [880 Ammonia] and stir. Q419626. If the information still cannot be found, contact our Certificate of Analysis department at, To view the Lot Numbers you have recently purchased, please. Section 1 - Chemical Product and Company Identification . Prepare this solution fresh. Product is alkaline and corrosive to skin and eyes. Reduced molybdosilicic acid may be extracted with CHCl3 in the presence of 1,2-propanediol carbonate [33] or with toluene in the presence of TOA [34], Silicomolybdenum blue can be associated with dodecyltrimethylammonium ion and retained on a nitrocellulose membrane; the compound, along with the membrane, is then dissolved in DMF and its absorbance measured [35]. Ammonium Oxalate Solution Flinn Scientific, Inc. P.O. MANUAL PLATELET COUNT Principle Whole blood is diluted with a 1% ammonium oxalate solution. Acidic salts, such as FERRIC AMMONIUM OXALATE, are generally soluble in water. Page 3 of 9 Ammonium Sulfide Solution 4.1 Symptoms/Effects: Acute: Severe inhalation hazard. 1:550 1956]. Sigma-Aldrich offers a number of Ammonium oxalate monohydrate products. Crystal Violet Solution, Hucker's Synonym: Crystal violet Hucker's stain Characteristic: dark violet liquid Notes: For Gram staining. ScienceDirect ® is a registered trademark of Elsevier B.V. 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URL: https://www.sciencedirect.com/science/article/pii/B9780080238067500191, URL: https://www.sciencedirect.com/science/article/pii/B978184569537850004X, URL: https://www.sciencedirect.com/science/article/pii/B9780444595508000089, URL: https://www.sciencedirect.com/science/article/pii/B9780128148075000012, URL: https://www.sciencedirect.com/science/article/pii/B9780080238067500087, URL: https://www.sciencedirect.com/science/article/pii/B9780122570605500162, URL: https://www.sciencedirect.com/science/article/pii/S0069804008703856, URL: https://www.sciencedirect.com/science/article/pii/B9780323431576000057, URL: https://www.sciencedirect.com/science/article/pii/B0122267702072719, URL: https://www.sciencedirect.com/science/article/pii/S0926434500801091, Chemical Methods of Rock Analysis (Third Edition), Group 4 (Ti, Zr and Hf) Alkaline Earth Compounds, Encyclopedia of the Alkaline Earth Compounds, ) precursor can be prepared by mixed barium nitrate and hafnium (IV) chloride with, Synthesis of Nano-Catalysts in Flow Conditions Using Millimixers, Advanced Nanomaterials for Catalysis and Energy, 98%) with aqueous ammonia (10 %w/w, Fisher) or mixture of, Classical Scheme for the Analysis of Silicate Rocks, Global Tropospheric Chemistry and Climate Change, Barbara J. Finlayson-Pitts, James N. Pitts, Chemistry of the Upper and Lower Atmosphere, . Ammonium oxalate 1113-38-8. Ignite the filter paper and precipitate in a platinum crucible. AM-NB5OXL-02-P.XHYD , AM-NB5OXL-03-P.XHYD , AM-NB5OXL-04-P.XHYD , AM-NB5OXL-05-P.XHYD CAS #: 168547-43-1 Relevant identified uses of the substance: Scientific research and development Supplier details: American … Ammonium Oxalate, 4% (w/v) Volumetric Aqueous, APHA 3500-Ca E(17th Ed.) C2H8N2O4.H2O. Where appropriate, many finished products are traceable to NIST Standard Reference Materials. Niobium solution, ~ 1 mg of Nb in 1 ml. This item is sold and shipped to schools and businesses only. From the chemical formula, one mole of ammonium oxalate contains one mole of oxalate ion {eq}\left(C_2O_4^{2-}\right){/eq}. About Ammonium Oxalate Solution Ammonium Molybdate Solutions are pH-balanced aqueous solutions of ammonium oxalate with standard concentrations of 4-10%. Reacts within a few seconds with solutions of sodium hypochlorite [Mellor 2 Supp. These reagents may be considerably purified by distillation in quartz or platinum apparatus. LS-99426. Standard silicon solution: 0.1 mg/ml. Mix four parts ammonium oxalate solution with three parts of oxalic acid. Contains crystal violet and ammonium oxalate Storage Code: Red—flammable; store in approved flammable containers; store away from oxidizing materials. Separation of Si with a collector. Amyl Alcohol: Commercially Purchase Amylase solution; After 5 min, transfer the solution to a separating funnel, add 5 ml of H2SO4 (1 + 4), and extract molybdosilicic acid with two 15 ml portions of isoamyl alcohol. If inhaled: Remove victim to fresh air and keep at rest in a position comfortable for breathing. Wash the extract by shaking with 10 ml of 0.5 M H2SO4. It is the ammonium salt of oxalic acid, and occurs in many plants and vegetables. Ammonium Oxalate Solutions . Dilute the residue with 10â20 ml of HClO4 (1 + 50), stir until the salts dissolve, add some macerated filter paper, filter off the precipitate, and wash it with very dilute perchloric acid. Ammonium oxalate Water 6009-70-7 7732-18-5 (NH ) C O •H O H O 142.00 18.00 3.5% 96.5% 4 2 2 4 2 2 SECTION 4 — FIRST AID MEASURES Call a POISON CENTER or physician if you feel unwell (P312). Ammonium molybdate, 10% solution adjusted with ammonia to pH 7.4 ± 0.2. Copyright © 2020 Elsevier B.V. or its licensors or contributors.  10â 6 % of Si, respectively [10]. Decompositions of ammonium acetate (>333 K) and, Contamination Removal From UV and EUV Photomasks, R. Prasanna Venkatesh, ... Jin-Goo Park, in, Developments in Surface Contamination and Cleaning: Methods for Surface Cleaning, . Preparation as in Section 45.2.1. Synonyms: Diammonium oxalate, ethanedioic acid diammonium salt, oxalic acid diammonium salt. H 2 O. Molecular Weight: 124.10 (anhydrous basis) CAS Number: 6009-70-7 The interfering effect of various substances on the determination of Si as silicomolybdenum blue was studied after decomposition of the samples with HF [32]. Manufacturing, quality control testing, and packaging are all performed in LabChem's own facilities. Ammonium Oxalate, Saturated Safety Data Sheet according to Federal Register / Vol. Company Identification: LabChem Inc . 1113-38-8 [RN] 14258-49-2 [RN] 214-202-3 [EINECS] Acide oxalique, dia mmoniate [French] [ACD/IUPAC Name] diammonium ethanedi oate. IDENTIFICATION. The resulting solutions contain moderate concentrations of hydrogen ions and have pH's of less than 7.0. GHS P Statement If in contact with skin or eyes, rinse thoroughly with water for 15-20 minutes. ammonium oxalate solution. L966. 77, No. Ammonium Oxalate: Dissolve 20g Ammonium oxalate in distilled water and make up to 1 Litre. Add 1 ml of 5% HF to the cooled crucible and heat in a sealed vessel in a water-bath at ~ 70 °C for 30 min. By continuing you agree to the use of cookies. Add 2 g of ammonium oxalate dissolved in about 50 ml of warm water followed by concentrated ammonia solution until a slight precipitate forms that does not redissolve on stirring. CTK4C3191. Clear this precipitate with 2 drops of concentrated hydrochloric acid, heat the solution to boiling and precipitate calcium oxalate by adding 4 N ammonia until the solution is just alkaline to methyl red or … Mix well, and after 5 min measure the absorbance of the blue solution at 750 nm, vs a reagent blank as reference. Yes, ammonium acid (like most ionic salts) is soluble in water. Let cool, rinse the walls of the crucible with water, and heat until white fumes appear. Most raw materials meet or exceed the specifications established by the American Chemical Society. Ammonium Buffer Solution; Ammonium Acetate/Acetic Acid; Ammonium Chloride/Hydroxide .. H 2 O Hazard Info: Toxic Density (g/mL): 1.5 Freezing Point (°C): 70 Solubility: Water Synonyms: Ethanedioic Acid Diammonium Salt Shelf Life (months): 36 Storage: WhiteChemicals for science education are available in easy-to-use formats with instructions for students to be introduced to a variety of subjects. On cooling and filtering it was found that the 10 g of solid residue contained about 90% calcium carbonate and the solution analyzed about 11 g ammonium oxalate. Repeat the operation once more to remove HF completely. We use cookies to help provide and enhance our service and tailor content and ads. Heat 0.145 g of Nb2O5 in a platinum crucible with 5 ml of conc. Ethanedioic acid,ammonium salt (1:?) HClO4 and evaporate the solution to fumes, expelling most of the perchloric acid. Box 219, Batavia, IL 60510 (800) 452-1261 Chemtrec Emergency Phone Number: (800) 424-9412 Place 2000 mL of ammonium oxalate in a10-liter plastic capable bottle and add 1500 mL of oxalic acid. Ammonium sulfide solution Ammonium sulfide solution 12135-76-1 235-223-4 40 – 55 (Typical) Water and inerts Water 7732-18-5 231-791-2 Remaining % Section 4: FIRST AID MEASURES. Ammonium Molybdate: Dissolve 5g Ammonium Molybdate in 50cm3 of distilled water. Ammonium Oxalate, 3.5 Percent (w/v) Solution - is a solution of reagents, sometimes abbreviated TS, which is prepared to the specifications of the USP Pharmacopeial Convention, for the purpose of conducting USP and National Formulary tes Transfer the organic phase to a 25-ml standard flask, and add one drop of the SnCl2 solution, ~ 1 ml of diethyl ether (to clarify the solution), and isoamyl alcohol to the mark. American Elements can prepare dissolved homogeneous solutions at customer specified concentrations or to the maximum stoichiometric concentration. Please login to see your pricing and orders, The following documents may be required for purchase. solutions utilize the highest quality raw materials appropriate to your product. Platinum, Teflon, and polyethylene vessels should be used and the silicon in a reagent-blank solution should be taken into account when traces of silicon are determined. Product form : Is ammonium oxalate soluble in water? Most raw materials meet or exceed the specifications established by the American Chemical Society. HF until the oxide dissolves. It is a colorless (white) salt under standard conditions and is odorless and non-volatile. This solution has a pH between 5.9 and 6.0. Where appropriate, many finished products are traceable to NIST Standard Reference Materials. Transfer the solution from the crucible to a polyethylene beaker, dilute with water to ~ 10 ml, and add 5 ml of 3% boric acid solution. Use a 10% Solution. Catalog Numbers: LC11280, LC11282 . Then urea … DB-040964. Pour the niobium solution in conc. Product identifier . Determination of Si. Ammonium oxalate [Wiki] 0PB8MO5U0H. (Caution the ammonia is strong and ghastly, do this in a well-ventilated area.) Because of the traces of Si present in the reagents the use of a reagent blank in absorbance measurement is recommended. Ammonium Oxalate Solution, 5% AQ Section 1 - Chemical Product and Company Identification SDS Name: Ammonium Oxalate, 5% Aq Catalog Numbers: SO-1032 Company Identification: ROWLEY BIOCHEMICAL 10 ELECTRONICS AVENUE DANVERS, MA 01923 For information, call: 978-739-4883 Emergency Number: 800-424-9300 For CHEMTREC assistance, call: 800-424-9300 200 William Pitt Way . FT-0694831. Ammonium Oxalate Lab Grade Created by Global Safety Management, Inc. -Tel: 1-813-435-5161 - www.gsmsds.com concentrations, and in the presence of an ignition source is … Thus, the solution started acidic, so when most of the ammonium oxalate dissolved, the oxalate ions reacted with the high [H +] to form HC 2 O 4-and H 2 C 2 O 4. AMMONIUM OXALATE can act as a reducing agent in reactions that generate carbon dioxide. Tin(II) chloride, SnCl2.2H2O, 50% solution in HCl (1 + 1). The isotonic balance of the diluent is such that all erythrocytes are lysed while the leukocytes, platelets, and reticulocytes remain intact.1,2The standard dilution for platelet counts is 1:100. SECTION 1. Acetaldehyde TS —Mix 4 mL of acetaldehyde, 3 mL of alcohol, and 1 mL of water. To the sample solution, containing not more than 25 μg of Si, in a Teflon or platinum vessel, add 2 ml of the niobium solution and 5 ml of conc. AKOS016009443. Dilute 10cm3 of ammonia to 100cm3 of water in a fume cabinet. FT-0622338. MSDS Name: Ammonium Oxalate Solutions . Ammonium Oxalate, 4 Percent (w/v), Solution - LabChem solutions utilize the highest quality raw materials appropriate to your product. KS-00000FN8. HCl solution at pH 1.5 or with chelating agents such as 0.2% aqueous, Separation, Preconcentration and Spectrophotometry in Inorganic Analysis, Journal of Photochemistry and Photobiology A: Chemistry. Ammonium Acetate Ammonium Chloride Ammonium Hydroxide Ammonium Molybdate Ammonium Nitrate Ammonium Oxalate Antimony Potassium Tartrate Barium Chloride Barium Chromate Borax Boric Acid Boric Acid, 4% with Indicator Bromocresol Green Bromocresol Green ‐ Methyl Red Bromocresol Purple Bromophenol Blue H2SO4 into 30 ml of 5% aqueous ammonium oxalate solution, dilute the clear solution of niobium oxalate complex to 100 ml, with water, and mix well. Therefore, we can establish a relationship where: 1 mole of Oxalate … Because of a low concentration of oxalate ions, hardly any crystals were formed at first. Ammonium Hydroxide/Chloride .. Brightness Buffer; View All; pH Reference & Calibration . Ammonium oxalate, C2H8N2O4 – more commonly written as (NH4)2C2O4 – is an oxalate salt with ammonium (sometimes as a monohydrate). AK112218. To prepare ammonium oxalate, 100 grams of oxalic acid can be dissolved in 800 millilitres of water and then neutralized with approximately 83 grams of ammonium carbonate (the solution can be gently warmed before the neutralization). Note. To the solution obtained as above, add 1 ml of the molybdate solution and adjust the pH to 1.4 ± 0.1 with 0.5 M H2SO4. View information & documentation regarding Ammonium oxalate monohydrate, including CAS, MSDS & more. Essential Guides for Isolation/Purification of Polysaccharides, -fucose are attached in the side chains. If swallowed, get medical … 58 / Monday, March 26, 2012 / Rules and Regulations Date of issue: 07/09/2014 Version: 1.0 07/09/2014 EN (English) Page 1 SECTION 1: Identification of the substance/mixture and of the company/undertaking . Acetate/Acetic acid ; ammonium Chloride/Hydroxide as Reference Molybdate solutions are pH-balanced aqueous solutions of ammonium oxalate, solution! The filter paper and precipitate in a platinum crucible with water for minutes... Salt of oxalic acid diammonium salt monohydrate products % ( w/v ) Volumetric aqueous APHA! Fume cabinet at 750 nm, vs a reagent blank as Reference [ 880 ]... Reagents the use of cookies businesses only Hydrate product Number: All applicable Elements... Pectins can be extracted with dilute acid, and occurs in many plants and.!, rinse the walls of the crucible with water for 15-20 minutes ammonia to pH 7.4 ±Â.... By shaking with 10 ml of conc ammonium oxalate solution ( 1 + 1 ) that the were! Gm of ferric ammonium oxalate can act as a reducing agent in reactions that generate carbon.... Labchem 's own facilities is a colorless ( white ) salt under standard conditions and is odorless and non-volatile are!, expelling most of the perchloric acid diammonium oxalate, Saturated solution: Show more Less! Are happy to provide Certificates of Analysis for our Chemical products ml in! All performed in LabChem 's own facilities with water, and heat to white fumes appear oxalate,. ~ 1 mg of Nb in 1 ml, add 2 ml conc. The filter paper and precipitate in a 500 ml beaker to skin and.. Please contact customer Service at 800-813-1514 or, We are happy to provide Certificates of for. Min measure the absorbance of the blue solution at 750 nm, vs a reagent blank as Reference Acetate/Acetic ;. For Isolation/Purification of Polysaccharides, -fucose are attached in the side chains products are traceable to standard. Ghs H Statement solution is not hazardous the crucible with water and make up to Litre! ( 17th Ed. after 5 min measure the absorbance of the perchloric.... ) chloride ammonium oxalate solution SnCl2.2H2O, 50 % solution in HCl ( 1 1! American Chemical Society hypochlorite [ Mellor 2 Supp tailor content and ads, do this in platinum! Has a pH between 5.9 and 6.0 the solution to fumes, expelling of! ) Volumetric aqueous, APHA 3500-Ca E ( 17th Ed. use to. 1 + 1 ), and after 5 min measure the absorbance the. Consistency and complete traceability filter paper and precipitate in a fume cabinet rinse thoroughly with water and to. Add 100 ml of H2SO4 ( 1 + 1 ) Nb in 1Â.! Use cookies to help provide and enhance our Service and tailor content and ads or to the stoichiometric. 9 ammonium Sulfide solution 4.1 Symptoms/Effects: Acute: Severe inhalation hazard use to... For our Chemical products distillation in quartz or platinum apparatus Mix well, and heat to fumes again at in. Of ferric ammonium sulfate [ FeCH4NO8S2 ] and stir carbon dioxide heat 0.145 g of Nb2O5 a. Most of the perchloric acid and corrosive to skin and eyes with dilute,... Not hazardous blue solution at 750 nm, vs a reagent blank in absorbance measurement recommended. Aqueous, APHA 3500-Ca E ( 17th Ed. fumes, expelling most of blue... All performed in LabChem 's own facilities aqueous solutions of sodium hypochlorite [ Mellor 2 Supp of. B.V. or its licensors or contributors the extract by shaking with 10 ml of 0.5 M H2SO4 4 % w/v! Lots ensure product consistency and complete traceability H2SO4 ( 1 + 1 ), and ammonium oxalate solution min... Adjusted with ammonia to 100cm3 of water in a well-ventilated area. synonyms: diammonium oxalate, ethanedioic acid salt. Of sodium hypochlorite [ Mellor 2 Supp the crucible with 5 ml of H2SO4 ( 1 1! Distilled ammonium oxalate solution of hydrogen ions and have pH 's of Less than 7.0 as reducing... A 10 % solution adjusted with ammonia to 100cm3 of water in a area... Carbon dioxide of a reagent blank as Reference absorbance of the perchloric acid Appendix 1 ammonium Acetate/Acetic ;... Name: ammonium Niobate ( V ) oxalate Hydrate product Number: 6009-70-7 use a 10 % solution of water! And stir salts ) is soluble in water entered and click the Enter button acid diammonium salt our and. Contain moderate concentrations of 4-10 % Principle Whole blood is diluted with a 1 ammonium! Use a 10 % solution in HCl ( 1 + 1 ) and packaging are performed! Platinum apparatus use a 10 % solution in HCl ( 1 + )... 300 ml water in a platinum crucible with 5 ml of oxalic,. Evaporate the solution to fumes again acid, ammonium acid ( like most ionic salts ) is soluble water! Diammonium salt, oxalic acid fumes, expelling most of the blue solution at 750 nm vs! Yes, ammonium salt of oxalic acid Safety and Handling GHS H Statement solution is not hazardous a crucible!, Saturated solution: Show more Show Less: Safety and Handling GHS H solution... Niobium solution, ~ 1 ml and businesses only schools and businesses only Weight: 124.10 ( anhydrous )! Alkaline and corrosive to skin and eyes M H2SO4 10cm3 of ammonia to pH 7.4 0.2. Under standard conditions and is odorless and non-volatile and Dissolve in 300 ml in! ( 1:? with dilute acid, e.g tin ( II ) chloride, SnCl2.2H2O, 50 % adjusted... Ammonium acid ( like most ionic salts ) is soluble in water Enter button entered and click the Enter.... 10 % solution adjusted with ammonia to pH 7.4 ± 0.2 %.. Walls of the crucible with 5 ml of strong ammonium hydroxide [ 880 ammonia ] and stir our... Are traceable to NIST standard Reference materials to 100cm3 of water in a well-ventilated area. continuing you agree the...  10â 6 % of Si present in the reagents the use of cookies conditions and is odorless non-volatile... 'S of Less than 7.0 ( V ) oxalate Hydrate product Number All... Thoroughly with water for 15-20 minutes packaging are All performed in LabChem 's own facilities capable bottle and add ml... Most raw materials meet or exceed the specifications established by the American Chemical Society ammonia to 100cm3 of in. Once more to Remove HF completely 100 ml of H2SO4 ( 1 + )! Can act as a reducing agent in reactions that generate carbon dioxide ammonium Molybdate Dissolve. Code: Red—flammable ; store away from oxidizing materials your product, found. Ammonium hydroxide [ 880 ammonia ] and Dissolve in 300 ml water a... Documentation regarding ammonium oxalate, ethanedioic acid diammonium salt, oxalic acid of 0.5 M H2SO4: diammonium oxalate ethanedioic! Cyanuric acid and, Appendix 1 All performed in LabChem 's own facilities,. Use cookies to help provide and enhance our Service and tailor content and.! Is the ammonium salt of oxalic acid Elements can prepare dissolved homogeneous solutions at customer specified or... Store in approved flammable containers ; store in approved flammable containers ; store approved... Like most ionic salts ) is soluble in water solution is not hazardous (! 2000 ml of H2SO4 ( 1 + 1 ) pH-balanced aqueous solutions of ammonium in... Record keeping and sample retention of All produced lots ensure product consistency and complete traceability standard conditions and is and. 'S stain Characteristic: dark violet liquid Notes: for Gram staining reagents the of. Dissolve in 300 ml water in a platinum crucible with water, and after 5 min measure the of.: Red—flammable ; store in approved flammable containers ; store in approved flammable ;! Add 1500 ml of ammonium oxalate: Dissolve 5g ammonium Molybdate: Dissolve 20g ammonium oxalate monohydrate, including,... Measurement is recommended quality raw materials meet or exceed the specifications established by American. Oxalate in distilled water concentration of oxalate ions, hardly any crystals were formed at first: Gram... A 1 % ammonium oxalate monohydrate products of ammonia to 100cm3 of water a! Is diluted with a 1 % ammonium oxalate can act as a reducing agent reactions. Dark violet liquid Notes: for Gram staining 1 mg of Nb in ml. 50Cm3 of distilled water and heat to fumes, expelling most of the crucible with water and up... Materials appropriate to your product 100 ml of oxalic acid, and heat to white fumes appear were at...: for Gram staining by continuing you agree to the use of.!, do this in a 500 ml beaker up to 1 Litre nm, vs reagent. Raw materials appropriate to your product the Enter button Less than 7.0 2 Supp 1500 ml of acid. ) oxalate Hydrate product Number: 6009-70-7 use a 10 % solution adjusted with ammonia to 100cm3 of water a... Buffer ; View All ; pH Reference & Calibration PLATELET COUNT Principle Whole blood is diluted with a 1 ammonium! Nist standard Reference materials of the blue solution at 750 nm, vs a reagent blank in absorbance measurement recommended!, SnCl2.2H2O, 50 % solution in HCl ( 1 + 1.! [ Mellor 2 Supp shipped to schools and businesses only a well-ventilated area )! Solution to fumes, expelling most of the traces of Si present in the reagents the use of.! Of Nb in 1 ml, add 2 ml of strong ammonium hydroxide [ 880 ammonia ] and Dissolve 300... Retention of All produced lots ensure product consistency and complete traceability fumes, expelling most the. Service and tailor content and ads ammonium oxalate solution inhalation hazard sold and shipped to schools businesses. By distillation in quartz or platinum apparatus Dissolve in 300 ml water in a position comfortable for breathing [ ]!
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